RELATÓRIO PARA AUXÍLIO DE

RELATÓRIO PARA AUXÍLIO DE PARTICIPAÇÃO EM EVENTO
Projeto Agrisus No: 922/12
Nome do Evento: "The 16th Meeting of the International Humic Substances Society"
Interessado : Josiane Millani Lopes
Instituição: ESALQ / USP – Depto de Ciência do Solo
Endereço: Av. Pádua Dias, 11
CEP: 13418-900
Cidade: Piracicaba
Fone: (19) 3417-2141 Ramal: 2141
E-mail: [email protected]
Estado: SP
Local do Evento: Zijingang Campus of Zhejiang University, Hangzhou, China.
Valor financiado pela Fundação Agrisus: R$4.500,00
Vigência: 09/09/2012 à 14/09/2012
RESUMO DE SUA PARTICIPAÇÃO:
O 16º Encontro Internacional de Substâncias Húmicas foi extremamente interessante,
pois trouxe discussões e novidades a respeito de temas como o conhecimento da formação e das
características da matéria orgânica, que é de vital importância para a compreensão das suas
propriedades e consequentes interações existentes no solo, sendo fundamental para a área da
sustentabilidade, afinal só é possível preservar efetivamente quando detemos o conhecimento
adequado. O evento reuniu vários especialistas no assunto que apresentaram de forma simples e
direta as novidades em relação ao tema e pontos sobre a conservação da matéria orgânica no
ambiente. Positivamente, minha participação nesse evento foi de grande importância para o
aprimoramento da minha formação acadêmica, estabelecimento de contato com pesquisadores
renomados nesta área, além de me proporcionar uma proveitosa experiência no exterior.
RELATÓRIO DA PARTICIPAÇÃO NO EVENTO:
1. INTRODUÇÃO:
Em condições de clima tropical, o Brasil acumula um volume expressivo de resultados
gerados por grupos de pesquisa em solos, o qual confere ao país uma posição de destaque na
área. Porém a maior parte desses estudos está quase sempre voltada para a fração inorgânica do
solo, ficando a fração orgânica quase sempre em segundo plano.
É de conhecimento geral que a matéria orgânica é responsável por uma série de
benefícios para o solo, seja química, física ou biologicamente. É sabido ainda que a busca
incessante por sistemas sustentáveis e produtivos pode ocorrer através do manejo adequado dos
recursos disponíveis ao mesmo tempo em que satisfaz as necessidades humanas, mantém ou
melhora a qualidade ambiental e conserva os recursos naturais. Gerenciar adequadamente o
ambiente em que vivemos e simultaneamente mantê-lo é um grande desafio que depende, em
escalas distintas, principalmente da compreensão da dinâmica da interação existente entre a
matéria orgânica e o papel que esta desempenha sobre o aproveitamento dos recursos naturais
renováveis, através da ciclagem do carbono, dos nutrientes e da energia presente nos sistemas
agrícolas.
Ainda hoje muito pouco se sabe sobre a natureza e as características da matéria orgânica
nos solos tropicais e subtropicais. Os efeitos das práticas de cultivo, manejo e conservação sobre
a matéria orgânica e, mais especificamente, sobre a formação e distribuição das substâncias
húmicas no solo não se encontram suficientemente estabelecidos Desta forma o conhecimento
aprofundado das características e das condições dessa matéria orgânica é de suma importância
para a compreensão e consequente conservação do solo.
O 16º Encontro Internacional de Substâncias Húmicas trouxe com as seções propostas,
discussões e novidades a respeito de temas como o conhecimento da formação, estrutura e
características da matéria orgânica, que é de vital importância para a compreensão das suas
propriedades e consequentes interações existentes no solo, entre outros temas relevantes já
listados acima.
2. PROGRAMA DO EVENTO:
Em anexo (Anexo 1).
3. RESUMO DE SEU TRABALHO APRESENTADO
Os solos de maior ocorrência nos ambientes genericamente chamados de restinga são os
Espodossolos, caracterizados pela presença de horizonte espódico (Bh ou Bhm). São poucos os
estudos científicos relacionadas à gênese destes solos em regiões tropicais, assim como há
poucos estudos detalhados avaliando as características e a composição química da matéria
orgânica (MO) presente nestes solos, bem como as suas relações com a transcorrência do tempo.
Os municípios paulistas de Cananéia e Bertioga foram selecionados para o desenvolvimento
desta pesquisa devido à presença de diferentes unidades sedimentares e de vegetação
remanescente. A caracterização dos ácidos húmicos (AH) extraídos dos horizontes dos diferentes
perfis de Espodossolos com o emprego de técnicas espectroscópicas como Espectroscopia de
Infravermelho com Transformada de Fourier (FTIR) e Fluorescência, foram realizadas com o
objetivo de se conseguir um maior detalhamento da matéria orgânica (MO) presente nesses solos
e, a partir daí, relacionar os resultados com a estabilidade do carbono e o tempo de residência
médio (TRM) da MO. A principal hipótese testada foi a de que os perfis com a MO com maior
TRM teriam os maiores conteúdos de compostos mais recalcitrantes. Neste âmbito, os principais
resultados relacionados com os objetivos foram: os perfis mais antigos foram os que
apresentaram as maiores concentrações de compostos mais recalcitrantes, principalmente nos
horizontes subsuperficiais (Bh e Bhm), essa inferência pode indicar que com a transcorrência do
tempo a MO presente tende a sofrer alterações na sua composição e se tornar mais recalcitrante.
O resumo expandido apresentado no evento está em anexo (Anexo 2).
4. CONCLUSÕES:
O evento foi muito importante para a minha formação acadêmica, pois possibilitou o
aprimoramento do meu conhecimento em relação ao tema, bem como uma interação direta com
alguns renomados pesquisadores da área. Pude interagir com outros estudantes, de partes
diferentes do mundo, que também estão se formando nessa área do conhecimento. A troca de
experiências, bem como o acúmulo de informações geradas durante o evento foi muito
importante para o meu crescimento acadêmico e pessoal. Dentre os diferentes temas que foram
abordados, houve uma sessão dedicada à área de Estrutura, Formação e Características das
Substâncias Húmicas e Matéria Orgânica, enfocando temas atuais e apresentando perspectivas
futuras da pesquisa, na qual participei por meio de uma apresentação de resumo expandido do
projeto que desenvolvi durante o mestrado e também na forma de pôster.
5. DEMOSTRAÇÃO FINANCEIRA DOS RECURSOS DA FUNDAÇÃO AGRISUS.
O recurso liberado pela Fundação Agrisus (R$4.500,00) foi utilizado inteiramente na
compra das passagens aéreas internacionais, as quais excederam o valor liberado, sendo a
diferença paga à parte. Segue em anexo o recibo da compra (Anexo 3).
6. DATA E NOME DO PARTICIPANTE.
12 de Outubro de 2012,
Josiane Millani Lopes
Anexo 1:
Tentative Program of IHSS 16
th
Sunday, September 9 , 2012 Zhejiang Zijingang International
Hotel
8:00
18:00
12:00
18:00
14:00
20:00
Registration and pickup of materials: Reception Hall
Set‐up posters: Authors are expected to have your poster ready by 18:00
pm on September 10
Lunch
Reception‐Welcome cocktail
Monday, September 10th, 2012 International Conference
Center, Zijingang Campus, Zhejiang University
Morning Half
Chair Person: Jianming Xu
Opening Session
8:30
9:30
Opening Ceremony
Welcome address: Governative and Academic
Authorities
Photographing
9:30
9:50
Coffee/Tea Break
Chair Persons: Ladislau Martin‐Neto and Renfang Shen
Keynote lectures
a,*
a,b
b
9:50
10:20
W illiam T. Cooper , Malak M.Tfaily , Jane E. Corbet ,
b
Jeffrey P. Chanton
a
Department of Chemistry & Biochemistry
b
Department of Earth, Ocean and Atmospheric Science; Florida
State
University, Tallahassee, FL 32306‐4390, USA
10:20
10:50
Correlating bulk optical spectroscopy and ultrahigh resolution
mass
spectrometry to determine the molecular composition of
dissolved
organic matter in Northern Peatlands
Donald L. Sparks, Chunmei Chen
Delaware Environmental Institute, University of Delaware,
Delaware,
USA, 19711
The role of mineral complexation and metal redox coupling in
carbon
cycling and stabilization
1
10:50
11:20
Lars Tranvik
Uppsala University, Sweden
Sequestration and loss of NOM in inland waters ‐ from micro‐scale
to global scale
11:20
11:50
Joseph J. Pignatello
The Connecticut Agricultural Experiment Station, 123 Huntington
St., New Haven, CT, USA
Role of natural organic matter as sorption suppressant in soil
12:00
14:00
Lunch
Afternoon Half
Session 1 Formation, structure and characteristics of HS and NOM
Chair Person: Jerzy Weber
Keynote lectures
a
a
b
14:00
14:30
J.A. González Pérez , F. J. González Vila , G. Almendros , H.
a
a
b
Knicker , J.M. de la Rosa , Z. Hernández
a
IRNAS CSIC. Avda. Reina Mercedes, 10, 41012Seville, Spain
bRevisiting
structural
provided
by Spain
analytical pyrolysis
MNCN CSIC.
Serrano insights
115bis, 41080
‐Madrid,
about humic substances and related bio and geopolymers
14:30
Oral
15:00
15:00
presentation
15:20
Xudong Zhang
Institute of Applied Ecology, CAS, China
Microbial derived soil organic matter (or Humus):
Significance, technology and perspective
Hernandez Soriano MC, Horemans B, Smolders E
Division of Soil and Water Management, Katholieke Universiteit
Leuven,
Kasteelpark Arenberg 20, 3001 Heverlee, Belgium
FTIR analysis of soil organic matter to link the turnover of
organic
inputs with carbon respiration rates
a
b
15:20
15:40
Michael H.B. Hayes , Roger S. Swift
a
Chemical and Environmental Sciences, University of Limerick, Ireland
b
Queensland Alliance for Agriculture and Food Innovation, The
University of Queensland, Australia
Lumping or splitting: Holistic or fractionation approaches to
studies of humic substances
15:40
16:00
Zaccone C , Pabst S , Miano TM , Shotyk W
a
Department of Agro Environmental Sciences, Chemistry and
Plant
a,*
b,c
d
e
b
Institute of Earth Sciences, University of Heidelberg, 69120
Heidelberg, Germany
c
BHP Billiton Iron Ore, Exploration Area C, Newman 6753, Western
Australia
d
Department of Biology and Chemistry of Agro Forestry and
e
Environment, University of Bari, 70126 Bari, Italy;
Department
of
Renewable Resources, University of Alberta, Edmonton, Alberta,
T6G
2H1, Canada
The fate of mineral particles in bulk peat and corresponding
humic
acids throughout an ombrotrophic bog profile: atmospheric
dust
depositions vs. mineralization processes
16:00
16:10
Coffee/Tea Break
Chair Person: Fusuo Zhang
Oral presentation
a,
b
a
16:10
16:30
Oleg Trubetskoj *, Lubov Shaloiko , Dmitrii Demin ,
c
Marchenkov , Olga Trubetskayab
a
Institute of Basic Biological Problems, Russian Academy of
Victor
Sciences, 142290, Pushchino, Moscow region, Russia
b
Branch of Shemyakin and Ovchinnikov Institute of Bioorganic
Chemistry, Russian Academy of Sciences, 142290, Pushchino,
c
Moscow region, Russia; Institute of Protein Research,
Russian
Academy of Sciences, 142290, Pushchino, Moscow region, Russia
Splitting of soil humic acid fluorescence on different fluorophores
16:30
16:50
E. Michael Perdue
Department of Chemistry, Ball State University, Muncie, IN 47306 U.S.A
Standard and reference samples of humic acids, fulvic acids,
and
natural organic matter from the Suwannee River, Georgia –
Thirty
years of isolation and characterization
16:50
17:10
Antonio Nebbioso, Alessandro Piccolo
Centro di Ricerca Interdipartimentale sulla Risonanza
Magnetica
Nucleare (NMR) per l'Ambiente, l'Agro‐Alimentare ed i Nuovi Materiali
(CERMANU), Università degli Studi di Napoli Federico II, Portici, Italy
Molecular understanding of a humic acid by “humeomic”
fractionation
and benefits from preliminary HPSEC separation
17:10
17:30
a
b
a,b
Guixue Song , Rajaa Mesfiou , Aaron Dotson , Paul
a,b*
b
Westerhoff , Patrick Hatcher
a
School of Sustainable Engineering and The Built Environment, Arizona
State University, Tempe, AZ 85287,USA
b
Department of Chemistry and Biochemistry, Old Dominion University,
Norfolk, VA 23529, USA
Sulfur containing molecules observed in hydrophobic and
amphiphilic fractions of dissolved organic matter by Fourier
transform ion cyclotron resonance mass spectrometry
17:30
17:50
a ,*
b
a
Du Changwen , He Zhongqi , Zhou Jianmin
a
Institute of Soil Science, Chinese Academy of Sciences, Nanjing
210008,
China
b
USDA ARS, New England Plant, Soil, and Water Laboratory, Orono,
ME
04469,
USA
Characterization of soil humic substances using mid
infrared
photoacousctic spectroscopy
17:50
18:10
a,b
a
a
a
a
Xiaomin Li , Liang Liu , Tong Xu Liu , Tian Yuan , Wei Zhang ,
a,*
a
b
Fangbai
Li , Shungui Zhou , Yongtao Li
a
Guangdong Key Laboratory of Agricultural Environment
Pollution
Integrated Control, Guangdong Institute of Eco‐Environmental and
Soil
Sciences, Guangzhou 510650, China
b
College of Natural Resources and Environment, South China
Agricultural
University, Guangzhou 510642, China
Effects of synthetic quinones as electron shuttles on geothite
reduction
and current generation by Klebsiella pneumoniae L17
18:10
20:00
Dinner
th
Tuesday, September 11 , 2012 International Conference
Center, Zijingang Campus, Zhejiang University
Morning Half
Chair Person: Paul Bloom
Keynote lectures
a,
a
b
a
8:00
8:30
N Hertkorn *, M Harir , BP Koch , B Michalke , Ph Schmitt
a
Kopplin
a
Helmholtz Zentrum Muenchen, German Research Center
Environmental Health, Institute of Ecological Chemistry,
Ingolstädter
for
Landstrasse 1, D 85764 Neuherberg, Germany
b
Alfred Wegener Institute, AWI, Am Handelshafen 12, D
27570
Bremerhaven, (Building Co 5), Germany
Elucidating the biogeochemical memory of the oceans by means
of
High resolution organic structural spectroscopy
Oral presentation
8:30
8:50
8:50
9:10
9:10
9:30
Chernysheva M.G., Badun G.A.
Lomonosov Moscow State University Dpt. Chemistry, Moscow
119991, Russia
HS protein associates in the aqueous/oil system: composition
and colloidal properties
a
a
b
b
Sen Dou , Song Guan , Guang Chen , Gang Wang
Department of Resource Science, College of Resource and
Environmental Science, Jilin Agricultural University, Changchun
130118,
China and
b
College of Life Science, Jilin Agricultural University, Changchun
China
130118,
Dynamics of formed humic acid and fulvic acid newly in
14
aggregates
with the addition of C labelled wheat straw in a Typic Hapludoll
of
northeast
China
a
Coffee/Tea Break
Session 2 HS/NOM and carbon sequestration
Chair Person: Gudrun Abbt Braun
Keynote lectures
a,b
b
b
9:30
10:00
Deborah P. Dick , Cecília S. Reis , Cimélio Bayer , Jennifer S.
b
Caldas
a
Institute of Chemistry, Federal University of Rio Grande do Sul
Ave. Bento Gonçalves, 9500, 91501‐970 Porto Alegre, Brazil
b
Soil Science Department, UFRGS, Brazil
Carbon sequestration in subtropical Oxisols profiles: retention
capacity
and effect of soil management
10:00
Oral
10:30
10:30
presentation
10:50
Jinshui Wu
Key Laboratory for Agro ecological Processes in Subtropical
Regions,
Institute of Subtropical Agriculture, CAS, Changsha, Hunan,
410125,
China
Dynamics in the microbial transformation of soil organic carbon
a
b
Agnieszka Medyńska Juraszek , Leszek Kuchar
a
Wroclaw University of Environmental and Life Sciences, Institute of
Soil
Science and Environmental Protection
b
Department of Mathematics, Grunwaldzka 53, 50 357 Wroclaw, Poland
Carbon sequestration rates in organic layers of soils under the
Grey
poplar (Populus x canescens) stands impacted by heavy metal
pollution
10:50
11:10
Liebner, F.,* Wieland, M., Hosoya, T., Pour, G., Potthast, A.,
Rosenau, T
University of Natural Resources and Life Sciences, Vienna, Department
of
Chemistry, Muthgasse 18, A 1190 Vienna, Austria
CO 2 sequestration by humic substances and the contribution
of quinones and quinone imines: Consideration on the molecular
scale
11:10
11:30
a
b
c
Raymond Liu , Jianming Xu , C. Edward Clapp
a
Retired Scientist, St. Paul, MN, USA
College of Environmental and Natural Resource Sciences,, Zhejiang
University, Hangzhou, 310029 China
c
Research Chemist & Professor, USDA ARS & U MN,St. Paul, MN, USA
b
Carbon sequestration in organic farming
11:30
11:50
a,b
a
a
a,
Ran Bi , Yong Yuan , Li Zhuang , Shungui Zhou *
a
Guangdong Institute of Eco‐environmental and Soil Sciences,
Guangzhou 510650, China
b
Guangzhou Institute of Geochemistry, Chinese Academy of
Sciences,
Guangzhou 510640, China
Electron transfer capacity as a rapid index for soil organic
carbon
stability
12:00
14:00
Lunch
Afternoon Half
Session 4 HS/NOM and the environmental processes of toxic elements
and anthropogenic organics
Chair Person: Irina Perminova
Keynote lectures
a,*
b
a
14:00
14:30
W illiam C. Koskinen , Alegria Cabrera , Kurt A. Spokas , Lucia
b
a
a
Cox , Jennifer L. Rittenhouse , Pamela J. Rice
a
USDA Agricultural Research Service, 1991 Upper Buford Cir., Rm.
439,
St. Paul, MN, USA
b
Instituto de Recursos Naturales y Agrobiología de Sevilla (IRNASE
CSIC),
P.O. Box 1052, 41080 Sevilla , Spain
Effect of carbonaceous soil amendments on potential mobility of
weak
acid herbicides in soil
Oral presentation
14:30
14:50
14:50
15:10
Haizhen Wang, Zhongzhen Liu, Yan He, Jianming Xu*
College of Environmental and Natural Resource Sciences, Zhejiang
Provincial Key Laboratory of Subtropical Soil and Plant Nutrition,
Zhejiang University, Hangzhou, 310058, P.R. China
Contribution of soil organic and inorganic components to
butachlor
sorption in soils
a,*
a
a
Masami Fukushima , Ryo Okabe , Ryo Nishimoto , Shigeki
a
b
a
Tsutomu
Fukuchi ,Sato , Motoki Terashima
a
Laboratory of Chemical Resource, Division of Sustainable
Resource
Engineering, Graduate school of Engineering of Hokkaido
University, Sapporo 060 8628, Japan
b
Geological Isolation Research and Development Directorate, Japan
Atomic Energy (JAEA), 433 Muramatsu, Tokaimura, Nakagun, Ibaraki
3191194, Japan
Sorption of pentachlorophenol to organo clay complexes prepared by
polycondensation reactions of humic precursors
15:10
15:30
a,
a
b
Louloudi, M *, Papastergiou, M. , Perlepes, S.P.
a
University of Ioannina, Department of Chemistry, 45100 Ioannina,
Greece
b
University of Patras, Department of Chemistry, 26504 Patras, Greece
Mechanisms of co catalytic action of humic Like additives on
pentachlorophenol oxidation by a Fe porphyrin catalyst
15:30
15:50
Chair
Person:
15:50
16:10
Coffee/Tea Break
Claudio Ciavatta
a,
a
a
Irena Twardowska *, Ewa Miszczak , Sebastian Stefaniak ,
Philippe
b
b
Schmitt‐Kopplin , Mourad Harir
a
Polish Academy of Sciences, Institute of Environmental
Engineering,
34, M. Sklodowska Curie St., 41819 Zabrze, Poland
b
German Research Center for Environmental Heath, Helmholtz Zentrum
München, Institut für Ökologische Chemie, Neuherberg, Gemany
Effect of humification and temporal alterations of
organogenic
waste(sewage sludge) properties on its sorption capacity for metals
16:10
16:30
a, b
a
b
N. S. Kudryasheva , A.S. Tarasova , E.S. Fedorova
a
Siberian Federal University, Krasnoyarsk, 660041, Russia
b
Institute of Biophysics SB RAS, Krasnoyarsk, 660036, Russia
Mechanisms of detoxification by humic substances
16:30
16:50
a
b,c
a
a
Z. Matar , G. Chebbo , M. Troupel , L. Boudhamane , E.
d
e
e
a
Parlanti , E. Uher , C. Gourlay and G.Varrault *
a
Université Paris Est, LEESU MA 102 – 61 av. du Gal de Gaulle,
94010
Créteil Cedex, France
b
France
Université Paris Est, LEESU UMR MA 102 ‐ F‐77455 Marne La Valle
c
Lebanese Univesity, Faculty Enginering, Lebanon, NH USA
d
Université de Bordeaux, CNRS, UMR 5805, EPOC‐LPTC, 351 cours
de la
Libération, 33405 Talence Cedex, France
e
IRSTEA, Unité Rech Hydrosyst & Bioprocédés, F‐92613 Antony, France
Influence of organic matter from urban effluents on trace metal
speciation and bioavailability in river under strong urban pressure
a,b
a
c
16:50
17:10
M. Elisabete F. Silva , L. Teixeira de Lemos , O.C. Nunes ,
b,*
A.C. Cunha Queda
a
Departamento de Ambiente, Escola Superior de Tecnologia e Gestão
e
b
Viseu; UIQA/Departamento de Ciências e Engenharia de
Instituto Superior de Agronomia, Universidade Técnica de
Lisboa;
c
LEPAE Departamento de Engenharia Química, Faculdade de
Engenharia,
Universidade do Porto
Correlation between humic like substances and heavy metals in
composts
17:10
17:30
Martina Klučáková*, Kristýna Nováčková
Materials Research CentreCZ.1.05/2.1.00/01.0012, Brno University
of
Technology, Faculty of Chemistry, Purkynova 118, 612 00, Brno,
Czech
Republic
Comparison of thermal and chemical stability of Cu‐humic
complexes
18:00
21:00
Banquet
th
Wednesday, September 12 , 2012 International Conference
Center, Zijingang Campus, Zhejiang University
Morning half
Session 8 Characterization and function of biochar in the environment
Chair Person: Jinshui Wu
Keynote lectures
a,
a
a
ba
8:00
8:30
Jeffrey Novak *, Keri Cantrell , Don Watts , Mark Johnson USDA
ARS CPRC, 2611 West Lucas Street, Florence, SC, 29501, USA,
bDesigning relevant biochars to revitalize soil quality: Current status
USEPA‐NHEERL, 200 Southwest 35th Street, Corvallis, OR, 97333,
and advances
8:30
9:00
Michael H.B. Hayes
Carbolea Research Group, Chemical and Environmental
Sciences, University of Limerick, Ireland
Relationships between biochar and soil humic substances
9:00
9:30
Renkou Xu
Institute of Soil Science, CAS, China
Effect of biochar incorporation on chemical properties of
variable charge soils from tropical and subtropical regions
Oral presentation
9:30
9:50
a,*
a
bc
b
Novotny EH , Auccaise R , Lima LB , Madari BE
a
Embrapa Soils, Rua Jardim Botânico, 1024, CEP 22460 000, Rio
de
Janeiro RJ, Brazil
b
Embrapa Rice and Beans, Caixa Postal 179, CEP 75375 000, Santo
Antônio de Goiás – GO, Brazil
c
Federal University of Goiás, Caixa Postal 131, CEP 74690 900,
Goiânia – GO
Characterisation of humic substances extracted from soil treated
with charcoal (biochar)
9:50
10:00
Coffee/Tea Break
Session 3 HS/NOM and biogeochemical cycling of nutrients
Chair Persons: Raymond Hozalski
Keynote lectures
10:00
10:30
Fusuo Zhang
China Agricultural University, Beijing China
Improving soil quality in intensive agriculture to ensure food
security and environmental quality simultaneously
10:30
11:00
Steve Banwart
University of Sheffield, UK
Planetary scale
Soil carbon flux and biological weathering from nanometric‐ to
Oral
11:00
Presentation
11:20
a
b
a
CR Butterly , JA Baldock , C Ta ng
a
Department of Agricultural Sciences, La Trobe University,
Melbourne
3086, Australia
b
CSIRO Sustainable Agriculture Flagship, CSIRO Land & Water,
PMB 2,
Glen Osmond 5064, Australia
Alkalinity generation by agricultural residues under field conditions
a,b
a
a
11:20
11:40
O. O. Adesanwo , M. T. Adetunji , S. Diatta
a
African Rice Center, International Institute of Tropical
Agriculture,
Ibadan, Nigeria
b
Department of Soil Science & Land Resources Management, Faculty
of
Agriculture, Obafemi Awolowo University, Ile Ife
Field assessment of humic substances effect on phosphate rock
solubilzation
11:40
12:00
Dhanasekaran. K, Priyarani. R
Department of Soil Science and Agricultural Chemistry, Faculty
of
9
Agriculture, Annamalai University Annamalai nagar‐608002,
Tamilnadu,
India
Effect of calcium boro humate application on the yield performance
of
cotton
12:00
14:00
Lunch
Afternoon Half
Session 5 HS/NOM, naturally occurring and engineered nanoparticles
Chair Persons: Baoshan Xing (Coordinator of Section 5) and Nicola Senesi
Keynote lectures
14:00
14:30
Baoshan Xing
The University of Massachusetts, Amherst, MA 01003, USA
Environmental processes and biotoxicity of engineered nanoparticles
14:30
Oral
15:00
15:20
15:00
Presentation
15:20
15:40
Perminova IV
Department of Chemistry, Lomonosov Moscow State University, Moscow,
Russia
Humic substances assisted synthesis of nanoparticles in the nature
and
in the lab
Ilya Lerman, Yona Chen, Benny Chefetz
Department of Soil and Water Sciences, Faculty of Agriculture, Food
and
Environment, The Hebrew University of Jerusalem, P.O. Box 12,
Rehovot
76100, Israel
Adsorption of contaminants of emerging concern by
carbon
nanotubes: influence of dissolved organic matter
a
a*
a
b
Di Zhang , Bo Pan , Hao Li , Baoshan Xing
a
Faculty of Environmental Science & Engineering, Kunming University
of
Science & Technology, Kunming, China, 650093
b
Department of Plant, Soil and Insect Sciences, University of
Massachusetts, Amherst, MA 01003
Adsorption of sulfamethoxazole
nanotubes
15:40
16:00
a
a
b
on
DOM suspended carbon
a
Vidali M S , Vlastos D , Bletsa E , Deligiannakis Y
a
Department of Environmental and Natural Resources Management,
University of Western Greece, 30100 Agrinio, Greece
b
Department of Materials Science and Engineering University of
Ioannina Greece
Genotoxicity study of multi walled carbon nanotubes in the
presence
of humic acids
16:00
16:20
a,
a
Graziele da Costa Cunha *, Daniel Felix Dias dos Santos ,
Luciane Pimenta Cruz Romão b, Zélia Soares Macedo
a
Departamento de Engenharia de Materiais; b Departamento de
c
Química; Departamento de Física, Universidade Federal de
Sergipe,
49100 000 São Cristóvão, SE, Brazil
Application of natural organic matter in the biosynthesis of αalumina
nanoparticles: the humic sol gel route
16:20
16:40
a
a,b
a
a
a,b,*
Xiaoli Tian , Kun Yang , Yong Xu , Huifeng Lu , Daohui Lin
Department of Environmental Science, Zhejiang University,
Hangzhou
310058, China
b
Zhejiang Provincial Key Laboratory of Organic Pollution Process and
a
Control, Zhejiang University, Hangzhou 310058, China.
Effect of humic acids on the physicochemical property and
Cd(II)
sorption of multiwalled carbon nanotubes
16:40
16:50
Coffee/Tea Break
Special Performance for Student Travel Award Grantees
Chair Persons: Teodoro Miano
Oral presentation
a,b*
b
a
16:50
17:05
H.M.Abdelrahman , D.C.Olk , C.Cocozza , D.
c
d
a
Ventrella , F.Montemurro , T. Miano
a
Department of Biology and Chemistry of Agro Forestry and
Environment, University of Bari, Italy
b
USDA ARS National Laboratory for Agriculture and the
Environment,
Ames, IA, USA
c
Research Unit for Cropping Systems in Dry Environments (CRA
SCA).
Bari, Italy
d
Research Unit for the Study of Cropping Systems (CRA SSC).
Metaponto,
Italy
Integrated physical chemical procedure for soil organic carbon
fractionation and characterization during transition to organic
farming
17:05
17:20
17:20
17:35
Olena Samsoni To dorova*, Natalia Klymenko, Liudmyla Savchyna
Institute of Colloid Chemistry and Chemistry of Water, National
Academy
of Science of Ukraine, 42 Vernadsky Avenue, Kyiv, 03680, Ukraine
Production of biologically stable safe drinking water from polluted
surface water sources
a,b,c
a,b,c,*
a
d
a
Ta o Jiang , Shiqiang Wei
, Xuemei Li , Song Lu , Meijie Li
Chongqing Key Laboratory of Agricultural Resources and
Environment,
Chongqing 400715, China
a
b
College of Resource and Environment, Southwest University,
Chongqing
400715, China
c
Engineering Research Center for Agricultural Non‐Point Source
Pollution
Control in the Three Gorges Reservoir Area, Chongqing 400715, China
d
Department of Applied Chemistry, Chongqing Vocational Chemical
and
Industry School, Chongqing 400020, China
Determination and characterization on the capacity of humic acid
for
the reduction of divalent mercury
17:35
17:50
17:50
18:05
Tadini, A. M., Moreira, A.B., Bisinoti, M.C.
Instituto de Biociências, Letras e Ciências Exatas, Department
of
Chemistry and Environmental Sciences, Universidade Estadual
Paulista
“Júlio de Mesquita Filho” São José do Rio Preto, São Paulo, Brazil
Influence of Aquatic Humic Substances from a sugarcane area and
orange in the dynamics of chromium ions in the environment
a
a,b
Anna S. Ta rasova , Nadezhda S. Kudryasheva
Siberian Federal University, Krasnoyarsk, 660041, Russia
b
Institute of Biophysics SB RAS, Krasnoyarsk, 660036, Russia
Reaction rates in enzymatic assay system in solutions of metal
salts
and humic substances
a
18:05
19:30
Dinner
Zhejiang Zijingang International Hotel
Chair Persons: Teodoro Miano and Ladislau Martin Neto
19:30
21:30
Celebrating 30th IHSS Anniversary
th
Thursday, September 13 , 2012
Conference Tour: Field trip and West Lake
th
Friday, September 14 , 2012 International Conference Center,
Zijingang Campus, Zhejiang University
Morning half
Session 7 HS/NOM in water and water treatment
Chair Persons: Fritz Frimmel
12
Keynote lectures
8:00
8:30
Oral presentation
8:30
8:50
Itamar Nadav, Jorge Tarchitzky, Yo na Chen*
Faculty of Agriculture, Food and Environment Hebrew University
of
Jerusalem, POB 12, Rehovot, Israel
Water repellency induced by organic matter (OM) in
treated
wastewater (TWW) infiltration ponds and irrigation
a,*
b
c
V irender K. Sharma , Jia Qian Jiang , and Hyunook Kim
a
Center of Ferrate Excellence and Chemistry Department, 150 West
University Boulevard, Melbourne, Florida, USA
b
School of Engineering and Built
Environment,
Glasgow
Caledonian University, Cowcaddens Road, Glasgow, Scotland, G4
0BA, United Kingdom
c
University of Seoul, Dept. of Environmental Engineering, 90
Jeonnong dong Dongdaemun gu, Seoul 130‐743, Korea
Ferrate(VI): Novel compound for removal of natural organic
matter in
water
8:50
9:10
Rolf D. Vogt*, Alexander Engebretsen, Christian Mohr
Department of Chemistry, University of Oslo, Norway
The effect of increased Dissolved natural organic matter
eutrophication
on
9:10
9:30
Fuqiang Liu
Nanjing University, Nanjing, 210046, China
Efficient removal of DOM and high purification of wastewater by
anovel magnetic polymer microspheres technology: Investigation and
application
9:30
9:50
Lingling Wang , Longfei Wang , Xuemei Ren , Xiaodong Ye ,
a
a
a
a
a
Wenwei Li , Shijie Yuan , Min Sun , Guoping Sheng , Hanqing Yu ,
ca
Xiangke Wang Department of Chemistry
b
Department of Chemical Physics, University of Science & Technology
of
China
a
a
c
c
b
Institute of Plasma Physics, Chinese Academy of Sciences, Hefei,
230026,
China
pH dependence of configurations and surface properties of
microbial
extracellular polymeric substances (EPS)
9:50
10:00
Coffee/Tea Break
Session 6 HS/NOM, biodiversity and ecosystem health
Chair Persons: Roger Swift
Keynote lectures
10:00
10:30
a,*
b
Phil Brookes , Sarah Kemmitt
*
Sustainable Soils and Grassland Systems, Rothamsted
Research,
Harpenden, Herts AL5 2JQ UK.
b
Current address: FSA, London, E14 5HS.
How important is microbial biodiversity in
mineralization of soil organic matter?
10:30
11:00
controlling the
Fengchang Wu
Chinese Research Academy of Environmental Sciences, Beijing, China
Natural organic matter and its environmental effects in Chinese lakes
Oral
11:00
Presentation
11:20
a
a,b,*
a, c
Yan Li , Wenfeng Ta n , Luuk K. Koopal
a
College of Resources and Environment, Huazhong Agricultural
University,
Wuhan 430070, China.
b
State Key Laboratory of Soil Erosion and Dryland Farming on the
Loess
Plateau, Institute of Soil and Water Conservation, Chinese Academy
of
Sciences & Ministry of Water Resources, Yangling, Shanxi 712100,
P.R.
Chin.
c
Laboratory of Physical Chemistry and Colloid Science, Wageningen
University, 6703 HB Wageningen, The Netherlands.
The influence of humic acids on the activities of lysozyme and urease
*
11:20
11:40
Millour M., Gagné J.P.
Institut des sciences de la mer de Rimouski, Université du Québec
àRimouski, 310 Allée des Ursulines, G5L 3A1, Rimouski, Québec, Canada
Sorption between humic substances and marine microalgae in
estuaries: effects of microalgae species, pH and salinity
11:40
12:00
Prabhat Pramanik, Pil Joo Kim
Division of Applied Life Science, Gyeongsang National University,
Jinju,
660701, South Korea
Feasibility of chelating agent utilization for suppressing methane
production during soil organic matter decomposition
12:00
14:00
Lunch
*
Afternoon half
Session 9 Industrial products and application of HS
Chair Persons: Dan Olk (Coordinator of Section 9) and Xuedong Zhang
Keynote lectures
a
a
b
b
14:00
14:30
Dan C. Olk , Dana L. Dinnes , Chad Callaway , Mike Raske
a
USDA ARS, National Laboratory for Agriculture and the Environment,
Ames, IA 50011, USA
b
Innovative Crop Solutions, Radcliffe, IA, 50230, USA.
On farm evaluation of a humic product in Iowa (U.S.) maize production
Oral presentation
14:30
14:50
14:50
15:10
a
a
b
c
a
Traversa A , Loffredo E , Palazzo AJ , Bashore TL , Senesi N
a
Dipartimento di Biologia e Chimica Agro‐forestale e
Ambientale,
University of Bari, 70126 Bari, Italy
b
ERDC CRREL, Hanover, NH 03755 1290, USA;
c
HQ ACC/A3A, Airspace, Ranges, Airfield Operations Division, Langley
AFB,
VA 23665 2789, USA.
Enhancement of germination and early growth of different
populations
of switchgrass (Panicum virgatum L.) by compost humic acids
a
a,*
Guido Meyer , Renate Klöcking
a
Institut für Verfahrensentwicklung, Torf und Naturstoff‐Forschung,
Zittau/Görlitz, Zittau, Germany.
Friedrich Schneider‐Straße 26, D‐02763 Zittau, Germany;
Humic acid quality: 2. Using oxalic acid as precipitating agent
a
b
c
c
a
15: 10
15:30
Karaman MR , Turan M , Tutar A , Dizman M , Şahin S
aDepartment of Soil Sci. and Plant Nutrition, Agri.
GaziosmanpasaFaculty,
Univ, Tokat, Turkey
bDepartment of Soil Sci. and Plant Nutrition, Agri. Faculty, Ataturk
Univ,
Erzurum, Turkey
cDepartment of Chemistry, Faculty of Sci., Sakarya Univ, Sakarya,
Turkey
Possible use of leonardite based humate sources as a potential
organic fertilizer
15:30
15:50
Jingdong Mao , Dan C. Olk , Na Chen , Dana L. Dinnes , Mark
c
Chappell
a
Department of Chemistry and Biochemistry, Old Dominion
University,
Norfolk, VA, 23529, USA
b
USDA ARS, National Laboratory for Agriculture and the
Environment,
Ames, IA 50011, USA
a
b
a
b
c
U.S. Army Corps of Engineers, 3909 Halls Ferry Rd., Vicksburg, MS
39180,
USA
Chemical properties of humic and fulvic acid products and their ores
of
origin
15:50
16:10
a
b
c
Richard Lamar , Dan C. Olk , Lawrence Mayhew , Paul R. Bloom
a
EarthFax Development Corp., 1770 N. Research Park Way, North
Logan,
d
UT 84341, USA
b2110 University Blvd, Ames, IA, 50011, USA
USDA‐ARS, National Laboratory for Agriculture and the
c
3899 Schreiner Rd, Spring Green, WI, 53588, USA
University of Minnesota, 1991 Upper Buford Circle, St. Paul, MN
55108,
USA
Evaluation of a proposed standardized analytical method for
the determination of humic and fulvic acids in commercial products
d
16:10
16:30
Mora, V., Jannin, L., Bacaicoa, E., Arkoun, M., Fuentes, M.,
Olaetxea, M., Baigorri, R., Garnica, M., San Francisco, S.,
Zamarreño, AM., Ourry, A., Etienne, P., Laîné, P., Yvin, JC., García
Mina, JM
INRA, UMR 950 Ecophysiologie Végétale, Agronomie et nutritions N, C,
S. Esplanade de la paix, 14032 Caen Cedex, France
CIPAV Roullier Group Poligono de Arazuri Orcoyen, Calle C, n°32, E
31160
Orcoyen, Spain
DEPARTMENT of Chemistry and Soil Chemistry. University of
Navarra. CRIAS Roullier Group 55 boulevard Jules Verger, 35800
Dinard, France Potential direct mechanisms involved in the action of
humic substances on plant development
16:30
16:40
Steve Azzarello
Humic Products Trade Association
The humic products trade association: Its activities and plans
Closing Ceremony
16:40
17:00
18:00
20:00
Concluding remarks by Jianming
Xu
Dinner
Anexo 2:
Humic substances of spodic horizons in the coastal plain of São Paulo
State
Lopes JMa*, Vidal-Torrado Pa, Buurman Pb, Camargo PBa
a
Departamento de Ciência do Solo, Escola Superior de Agricultura “Luiz de Queiroz”, Universidade de São Paulo.
Av. Pádua Dias, 11, C.P. 9, Bairro Agronomia, Piracicaba, SP. CEP 13418-900, Brazil b Dept. of Environmental
Sciences, Wageningen University. P.O. Box 47, 6700 AA Wageningen, The Netherlands.
*Tel. No. +55-19 3417 2141; E-mail: [email protected]
Keywords coastal plain; humic substances; mean residence time; Podzol; soil organic matter; spodic horizons
Abstract The most common soils that occurred in environments generically called restinga are Podzol that are
characterized by the presence of spodic horizon (Bh or Bhm). There are few scientific studies related to the genesis
of these soils in tropical regions, and there are few detailed studies assessing the chemical characteristics and
composition of organic matter (OM) present in these soils, as well their relations with time. The cities Cananéia and
Bertioga were selected for this research due to the presence of different sedimentary units and remaining vegetation.
The characterization of humic acids (HA) was realized using spectroscopic techniques like Fourier Transform
Infrared spectroscopy (FTIR) and fluorescence. Samples were extracted from different Podzol horizons in order to
achieve more details about the OM present in these soils and relate the results to the stability of carbon and the
mean residence time (MRT) of OM. The main hypothesis tested was that the profiles were the OM has less TRM
would have the highest contents of more recalcitrant compounds. In this context, the main results related to the
objectives were: the older profiles were those with the highest concentrations of more recalcitrant compounds,
especially in the subsurface horizons (Bh and Bhm). This inference may indicate that with transcurrent of time MO
tends to undergo changes in its composition and become recalcitrant.
Introduction
The OM plays a fundamental role in the Podzol
formation process, consisting of humic substances
(HS), that are products of oxidative degradation and
subsequent humification of OM (Stevenson, 1994).
The HS are organic substances chemically complex,
amorphous, generally dark, hydrophilic, acidic or
partially aromatic (Schnitzer, 1982) composed by
compounds that have a wide variety of functional
groups (carboxylic, hydroxyl, phenolic, carbonyl,
etc.). Part of the HS present in the Bh horizons and
Bhm comes from the superficial OM decomposition
and some authors have suggested that the TMR
estimated by 14C and, consequently, the stability of
OM in the soil increases with depth (Paul et al, 1997).
The study of SH is possible using spectroscopic
techniques such as FTIR (González-Pérez et al.,
2008), which permits the study of the structure of HS.
Another technique widely used is the fluorescence, by
which it is possible to estimate the humification
degree (Milori et al., 2002), allowing the elucidation
of different aspects of reactivity and chemical
structure of OM.
Materials and methods
The profiles called P03, P10 and P30 are located in
Cananéia, and the profile P04 in Bertioga. FTIR
measurements were performed using methods well
established in the literature (Stevenson, 1994) using
tablets with 1 mg of SH and 100 mg KBr. For
preparation of the tablets, samples were ground with
KBr, packed in a mold and pressed. The spectra were
obtained using 16 scans in the range 4000-400 cm -1,
with spectral resolution of 4 cm and a range of 1 cm-1.
For fluorescence analysis, the HA extracted from the
soil profiles were dissolved in NaHCO3 solution 0.05
mol L-1. The spectra were obtained according to the
methodology proposed by Milori et al. (2002).
For the dating of the soil source material (coastal
sediments) by thermoluminescence (TL), the samples
were collected with the aid of black PVC pipe inserted
horizontally to the ground surface. Both the collection
and the dating were performed according to the
procedures cited by Tatumi et al. (2003).
Results and discussion
The FTIR spectra of HA extracted from different
horizons (A, Bh and Bhm) from the profiles P03, P04,
P10 and P30 are shown in Figure 1. Is possible to
observe that the spectra of HA extracted from different
soil profiles show similarities. There are no significant
structural and chemical variations between samples in
AH, but it is possible to observe changes in the
intensities between the groups in each profile.
Fig. 1 FTIR spectra of HA extracted from the surface horizons (A) and subsurface (Bh and Bhm) from P03, P10, P30
and P04 profiles, respectively.
In the spectra of all profiles can be observed that
samples of the soil surface have an absorption band
between 1170 - 950 cm-1, the same being absent in the
spectra obtained for the subsurface layers Bhm and
Bh. This band is assigned to CO stretching of
polysaccharides. This result is related to higher
content of OM decomposed or even by the presence of
microbial activity. It is well know that microorganisms
produce polysaccharides during the decomposition of
OM (Stevenson, 1994). Another region of the
spectrum can be observed only for the samples of the
soil surface is between 1660 - 1630 cm -1 which is
attributed to stretching of C = O from amide, which
can usually be associated with proteins.
In the spectral region between 3400 - 3300 cm -1, the
absorption due to stretching of the H-bound to OH and
NH is stronger in samples from the surperficial
horizons, and the lower intensity is observed for Bh
horizons. Another variation in intensity is observed in
the region between 2940 - 2900 cm -1, which is
assigned to CH stretching of aliphatic groups, being
observed a greater intensity of this band in the soil
surface, showing a higher concentration of aliphatic.
Another variation in depth may be observed in the
spectral region between 1725 - 1720 cm -1 in which the
absorption is due to stretching C = O of COOH, being
observed a greater intensity in the subsurface horizons.
A reverse trend can be observed in the region of the
spectrum between 1280 - 1200 cm -1, in which
absorption may be due to CO stretching of aryl-ethers
and/or phenolic. The greater intensity of this band
occurs in the spectra of samples from subsurface
horizons, showing a higher concentration of phenolic
compounds in depth. The intensities of the band
assigned to aliphatic CH stretching region of the
spectrum between 1460 - 1450 cm-1 showed a slight
increase for the samples of surface horizons, with
almost imperceptible difference in intensity of this
band for the samples of Bh and Bhm horizons.
In general, the results suggest an increasing degree of
humification of OM in depth, as evidenced by the
presence of more condensed compounds in the
subsurface layers and the highest concentration of
aliphatic compounds and the presence of
polysaccharides in the surface horizons.
The results of fluorescence showed that the greatest
degree of AH humification were obtained for the Bh
horizons of the profiles P03 and P30 in relation to the
profiles P10 and P04. The lower degree of
humification was determined in HA from the surface
horizons of all profiles. The degree of humification is
related to the presence of compounds with more
complex structures such as aromatic compounds.
Looking at Figure 2, the samples that have higher rates
of humification are the ones with the higher content of
more recalcitrant compounds. Some studies suggest
good correlations between the humification rate
obtained by fluorescence spectroscopy and other
techniques to achieve results directly or indirectly
related to the stage of humification of OM evaluated
(Milori et al., 2002).
The results obtained by fluorescence showed the same
trend of humification was maintained for the different
horizons of the different profiles. Comparison between
the profiles showed the same results obtained by
FTIR. The P30 is the profile that has the highest rates
of humification in relation to others.
Fig. 2 Index A465 obtained from fluorescence spectra
of HA extracted from P03, P10, P30 and P04 profiles,
according to Milori et al., (2002).
Tabela 1 – Age of the sediment by TL
Sample
P03 Bhm1
P10 Bhm
P30 Bhm
1
2
Depth
(cm)
Age of material
TL1 (years)
120-142
117-150
58-105
131.500 ± 15.100
41.200 ± 3.400
271.000 ± 85.300
TRM
(years
B.P.) 2
9.600
4.260
18.500
TL – Termoluminescência
B.P. – Before Present
By evaluating the results of fluorescence and
comparisons made with the results of FTIR and dating
was possible to establish a positive relationship
between the transcurrent time and humification of the
HS. Considering only the TRM of OM was possible to
conclude that the older the profile, more stable the OM
present in it.
Further investigation about the stability of OM and its
comparisons with other factors that influence this
process should be made, since there is a need for
greater understanding in the concentrations of OM as
well its preservation in soil.
References
González-Pérez M, Vidal-Torrado P, Colnago LA,
Martin-Neto L, Otero XL, Milori DMBP, Gomes
FH 2008 13C NMR and FTIR spectroscopy
characterization of humic acids in spodosols under
tropical rain forest in southeastern Brazil.
Geoderma. 146, 425-433.
Milori DMBP, Martin-Neto L, Bayer C, Mielniczuk J,
Bagnato VS 2002 Humification degree of soil
humic acids determined by fluorescence
spectroscopy. Soil Science. 167, 739-749.
Paul EA, Follett RF, Leavitt SW, Halvorson A,
Peterson GA, Lyon DJ 1997 Radiocarbon dating
for determination of soil organic matter pool sizes
and dynamics. Soil Sci. Soc. of Am. J. 61, 1058–
1067.
Schnitzer M 1982 Organic matter characterization. In:
Methods of soil analysis: Chemical and
microbiological properties. Madison: ASA-SSSA.
582-594.
Stevenson FJ 1994 Humus chemistry: genesis,
composition, reactions. Jonh Wiley, New York,
USA.
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